Synthesis of BIS(2.2,2-Trifluoroethyl) vinylphosphates

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Title:	Synthesis of BIS(2.2,2-Trifluoroethyl) vinylphosphates
Author:	Stock, Joseph R.
Description:	The focus of the research presented here is the synthesis, isolation and characterization of vinyl phosphates containing the bis(2,2,2-trifluorethyl) group. The first step involved the synthesis of bis(2,2,2-trifluoroethoxy) phosphorochloridate. This reagent was then added to a ketone enolate, formed by the reaction of LDA, prepared in situ from diisopropylamine and η-butyllithium, and a cyclic ketone to yield the desired vinyl phosphates.
Permanent Link:	http://rave.ohiolink.edu/etdc/view?acc_num=ysu997203540 http://hdl.handle.net/2374.OX/3123
Date:	1998

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Now showing item 11 of 204